Jag har testat en gång.
Har inget minne ifrån händelsen direkt, har vaga minnen från den veckan överhuvudtaget, men tydligen så ska jag ha suttit i en fotölj, med en tulipan i handen (som jag plockat ur vasen på köksbordet) och suttit och fört en konversation med tulipanen och två av mina personligheter.
Fick för mig att jag skulle gå och spraya ner ett casino med rosa glitterspray och skriva "Piska pasta i ladan" på framsidan av casinot med en blyertspenna.
Sen somnade jag.
Om du har svaga minnen från den veckan, hur vet du då att det var PCP ?
PCP verkar roligt, läste typ 20 tripprapporter på erowid alldeles nyss.
Bara man doserar rätt verkar det vara lungt. Det fanns en hel del skräckhistorier, men sånt är kul det med!
Ja, det här gör du väl en eftermiddag innan du tar itu med skolläxorna?
METHOD 1. A mixture of 100 g of anhydrous ethylamine and 220 g of cyclohexanone is kept 16 hours, shaken with solid KOH, and the oil layer is removed by decantation. Distill the oil layer in vacuo to get the intermediate N-cyclohexylidenethylamine. Prepare a mixture of phenyllithium by mixing 11 g of lithium and 76 ml PhBr in 500 ml of Et20. Add the phenyllithium dropwise to a solution of 51 g of the N-cyclohexylidenethylamine in 500 ml of Et20, with stirring and cooling, to keep the temp at 0¡. Stir for one hour and then decompose by adding water. Separate the Et20 layer, wash with H20 and distill to get 1- phenylcyclohexylethylamine or analog. The hydrochloride form is obtained in the usual way, as given below.
METHOD 2. A mixture of 170 g of piperidine, 220 g of cyclohexylamine, and 750 ml of benzene is azeotropically distilled until the evolution of H20 stops, then vacuum distill to get cyclohexenyl-piperidine. p-toluenesulfonic acid monohydrate (190 g) in 250 ml of PhMe is heated under a water trap until all the H20 is removed, then add a solution of 165 g of cyclohexyl-piperidine in 500 ml of Et20, with cooling, to keep temp at 0¡. A solution of I mole of PhMgBr (made from 157 g of PhBr and 24 g of Mg) in 750 ml of Et20 is added (still holding the temp at 0¡ to 5¡). The mixture is stirred for an additional 30 min after the dropwise addition is complete. Decompose the mixture by adding an excess saturated NH4Cl and NH40H. The Et20 layer is removed, dried over K2CO3, and distilled to give phenylcyclohexylpiperidine. Convert to the hydrochloride form by dissolving the free base in an excess of iso-PrOH-HC1 and then precipitate the salt (the hydrochloride) with Et20 and crystallize from Et20-iso-PrOH (this is a mixture).
Ja, det här gör du väl en eftermiddag innan du tar itu med skolläxorna?
METHOD 1. A mixture of 100 g of anhydrous ethylamine and 220 g of cyclohexanone is kept 16 hours, shaken with solid KOH, and the oil layer is removed by decantation. Distill the oil layer in vacuo to get the intermediate N-cyclohexylidenethylamine. Prepare a mixture of phenyllithium by mixing 11 g of lithium and 76 ml PhBr in 500 ml of Et20. Add the phenyllithium dropwise to a solution of 51 g of the N-cyclohexylidenethylamine in 500 ml of Et20, with stirring and cooling, to keep the temp at 0¡. Stir for one hour and then decompose by adding water. Separate the Et20 layer, wash with H20 and distill to get 1- phenylcyclohexylethylamine or analog. The hydrochloride form is obtained in the usual way, as given below.
METHOD 2. A mixture of 170 g of piperidine, 220 g of cyclohexylamine, and 750 ml of benzene is azeotropically distilled until the evolution of H20 stops, then vacuum distill to get cyclohexenyl-piperidine. p-toluenesulfonic acid monohydrate (190 g) in 250 ml of PhMe is heated under a water trap until all the H20 is removed, then add a solution of 165 g of cyclohexyl-piperidine in 500 ml of Et20, with cooling, to keep temp at 0¡. A solution of I mole of PhMgBr (made from 157 g of PhBr and 24 g of Mg) in 750 ml of Et20 is added (still holding the temp at 0¡ to 5¡). The mixture is stirred for an additional 30 min after the dropwise addition is complete. Decompose the mixture by adding an excess saturated NH4Cl and NH40H. The Et20 layer is removed, dried over K2CO3, and distilled to give phenylcyclohexylpiperidine. Convert to the hydrochloride form by dissolving the free base in an excess of iso-PrOH-HC1 and then precipitate the salt (the hydrochloride) with Et20 and crystallize from Et20-iso-PrOH (this is a mixture).
Om ni vill se hur en person är på PCP kan jag rekomendera Steve-O´s film PCP saved my life den finns med på extramaterialet på Out on bail.
Skit rolig film, han kom inte i håg nånting av filmen, och har inte kollat på den efteråt heller =)
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