Citat:
Ursprungligen postat av claymann
Var fr jag tag i:
Safrole (160g)(sassafras oil, yellow camphor oil) (Natural/Essential Oil distributor)
Dimethylformamide (DMF) (350mL) (Diethylformamide or Formamide will work)
p-Benzoquinone (Quinone, Benzoquinone) (120g) (Photo Shop, or Chem supply)
Palladium Chloride (PdCl2) (2g) (Photo Shop, or chem supply)
Methylene Chloride (DiChloroMethane, DCM) (this can be distilled from automotive solvents (just go into Nationwise, PepBoys, Sears, AutoZone And read the labels) Or a Liter can be bought from a Chem supplier.)(Zip-Strip furniture polish remover)
Hg salt (1 gram of: HgCl2, Hg(NO3)2, Hg(OAc)2, HgCl, It can be anything, and 1g should last you a long time.)
Isopropyl Alcohol (IPA, Pharmacies 91% Isopropyl Alcohol will be available)(get +3L)(don't get the 70% stuff) (or you can get pure stuff from a chem supplier)
Epsom Salts (Magnesium Sulphate) (MgSO4) (grocery store/pharmacy) (Spread out on a cookie sheet, and bake in the oven at 200C for 3hr to dry them - pretty useless if you don't dry it)
Thick Al foil (heavy duty, or pie pans from the Grocery store)
Muriatic Acid (31.45% HCl)(Pool pH down, Driveway cleaner, ~3$/gallon)
Sodium Hydroxide (NaOH) (Drain Cleaner Crystals) (Read these labels, Get the stuff that is JUST NaOH.) (Red Devil Lye, Lye - Hardware Store)
Ammonium Chloride (NH4Cl) (Photo Store or Chem Supplier)
Paraformaldehyde (Hardware store) (called Mildewcyde or DiGas - made by the same people who brought you Damp-Rid - hint-hint)
Peanut oil (this is a high boiling oil that we will use as an oil bath on the hotplate/stirring plate combo)
Acetone (for cleaning your glass and crystal work-up) (Paint Section of Hardware Stores)
Xylene (for crystallization) (paint section - thinner - get it specifically)